Description
These are Glass Coil Condenser/Heat Exchanger of fused glass construction are used for cooling and condensation. These heat exchangers are made entirely of glass i.e. the exchange tubes are fused to the jacket.
This result in the following main advantage:
- No seal points between the shell and the coil.
- Outstanding corrosion resistance since borosilicate glass is the only wetted part and therefore.
- Optimum conditions for the production of extremely pure products.
Units of this type are supplied in various designs with exchange areas ranging from 0.3 to 15 m2. Larger areas can be obtained by combining several exchangers.
The construction, especially of the larger units incorporates all the features required for operational safety:-
- The weight of the coil bank is taken up by a fused-in-guide funnel, preventing overloading at the points of fusion to the jacket.
- A built in anti-water chamber in sizes 2.5 m2 and above. This buffers dynamic pressure surges which occur primarily on the start-up.
The maximum operating pressure in the coil is 3 bar gauge for the larger units. The heat exchangers are connected to the services via flexible hoses or bellows. This prevents the transmission of stress or vibration to the heat exchanger from the service pipework. Coil heat exchangers are used mainly for condensation, cooling and heating with heat transfer fluids. Heating with saturated steam is restricted to exchangers with a maximum area of 1 m2.
The overall heat transfer coefficients, k to be expected for units with an exchange area of 2.5 – 15.0 m2 are approximately as follows:-
Liquid- Liquid exchange k = 120 – 175 W/m2k.
Condensation k = 230 – 315 W/m2k
Bench Top Glass Reactors consists of :
⦁ Stand with base, drip tray, support rods, bosses and all clamps
⦁ Glass Reaction Vessel Lid
⦁ Vessel FEP O-ring seal and PTFE Collar
⦁ Stainless Steel Drip Tray
⦁ Vessel to Manifold Insulated Hoses with Quick-Release Connections
⦁ Lower Inlet Manifold + Drain
⦁ Upper Outlet Manifold + Vent
⦁ PTFE Stirrer Guide and Coupling
⦁ Two stainless steel Vessel Support Collars
⦁ Locking Rod for Support Rod Bosses
Application
⦁ Chemical synthesis
⦁ Extraction / evaporation
⦁ Purification / crystallization
⦁ Separation
⦁ cGMP API production
⦁ Peptide synthesis
⦁ Process development
⦁ Scale-up
⦁ Cryogenic reactions
⦁ Pilot plant /kilo lab
Reaction Vessel Features
⦁ Range of single and vacuum jacketed vessels from 500 ml to 5 litres
⦁ Process vessels to mimic larger scale plant or manufacturing reactors
⦁ Precision engineered borosilicate glass vessels
⦁ DN100 5 neck Glass Lid fits all Vessel sizes
⦁ Wide range of accessory glassware including condensers, dropping funnels
Cat. Ref. | DN | d/DN1 | L | L1 | Type | Actual | Cross | Free | Max. |
H.T.A. | Area | Coolant | Jacket | ||||||
m2 | Cm2 | Rate | Cap. | ||||||
kg/hr. | Litre | ||||||||
HE3/3.5* | 80 | 16 | 600 | 75 | A | 0.35 | 5 | 1300 | 2 |
HE4/5* | 100 | 19 | 600 | 75 | A | 0.5 | 30 | 2400 | 4 |
HE4/6 | 100 | 19 | 750 | 100 | A | 0.6 | 30 | 2400 | 6 |
HE6/10 | 150 | 25 | 600 | 100 | B | 1 | 52 | 2600 | 9 |
HE6/15* | 150 | 25 | 850 | 100 | B | 1.5 | 52 | 2600 | 11 |
HE9/25* | 225 | 25 | 800 | 110 | B | 2.5 | 125 | 3300 | 18 |
HE12/25 | 300 | 25 | 600 | 125 | B | 2.5 | 175 | 5700 | 25 |
HE12/40* | 300 | 25 | 900 | 125 | B | 4 | 175 | 5700 | 35 |
HE16/40 | 400 | 25 | 600 | 125 | B | 4 | 450 | 6200 | 60 |
HE16/50 | 400 | 25 | 700 | 125 | B | 5 | 450 | 6200 | 70 |
HE18/60 | 450 | 40 | 750 | 150 | C | 6 | 820 | 4800 | 100 |
HE18/80 | 450 | 40 | 900 | 150 | C | 8 | 820 | 6200 | 110 |
HE24/120 | 600 | 50 | 1250 | 300 | C | 12 | 1520 | 6200 | 265 |
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