Description

The Global Antico Sulphuric Acid Concentration Plant is a high-performance vacuum evaporation system engineered to concentrate dilute sulphuric acid streams — typically 20–70% H₂SO₄ from industrial processes — up to commercial concentrations of 96–98%+ w/w. The process exploits the boiling point elevation of H₂SO₄ under reduced pressure, allowing water removal at significantly lower temperatures than atmospheric evaporation, preserving equipment integrity and reducing energy consumption. The dilute acid feed is introduced into a falling-film or forced-circulation evaporator where vacuum is maintained by a two-stage ejector or liquid ring vacuum system. Water vapour liberated during evaporation is drawn off and condensed, while concentrated acid is progressively recycled through the evaporator until the target concentration is achieved.

Heat input to the evaporator is provided by steam, hot water, or waste heat via indirect heating through acid-resistant heat transfer surfaces — typically tantalum tube bundles, borosilicate glass, or silicon carbide (SiC) shell-and-tube exchangers. An acid-mist scrubbing system downstream of the vacuum condenser captures acid carry-over before non-condensable gas is vented. An integrated heat recovery loop — using condensate heat to pre-warm incoming dilute acid — improves overall thermal efficiency by 25–35%. The plant operates continuously with automatic concentration monitoring via inline density measurement or refractometry, and automatic feed/draw-off rate adjustment. Available capacities range from 500 kg/day to 50,000 kg/day of concentrated acid output. Optional crystallization prevention heating circuits are included for high-concentration operation above 93% H₂SO₄.

Benchtop reactor (1)

Key Features​

  • Vacuum evaporation enabling low-temperature concentration
  • Tantalum, SiC, or borosilicate glass heat exchangers
  • Acid-mist scrubbing system on non-condensable vent
  • Integrated heat recovery — condensate to feed pre-heat
  • Continuous operation with automatic concentration control
  • Inline density / refractometry monitoring and control
  • Automatic feed and draw-off rate control loop
  • Anti-crystallization heating circuits for >93% H₂SO₄
  • Forced circulation to prevent stagnant hot-spot formation
  • Complete acid-resistant MOC throughout wetted systems

Technical Specifications​

Output Concentration Up to 98%+ H₂SO₄
Feed Concentration 20% – 80% H₂SO₄ (dilute acid)
Capacity Range 500 – 50,000 kg/day output
Heat Transfer Material Tantalum / SiC / Borosilicate Glass
Evaporator Type Falling Film / Forced Circulation
Energy Recovery 25–35% via heat integration
Concentration Control Inline density / refractometry
Emission Control Acid mist scrubber on vent

Industrial Applications

  • Fertilizer grade sulphuric acid production and regeneration
  • Battery acid (electrolyte) concentration to specification
  • Rayon and textile fibre manufacturing
  • Metals processing and pickling acid recovery
  • Refinery spent acid regeneration programs
  • Industrial effluent ZLD — dilute acid recovery and reuse

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